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Thiodiglycol (TDG) is the predominant hydrolysis product of the chemical warfare agent sulphur mustard. The extraction of TDG was investigated using pressurized liquid extraction and the results compared for a variety of different solvents and soils. TDG was analysed underivatised by gas chromatography with a flame photometric detector. A mixture of methanol-water (9:1) , proved to be the most efficient extracting solvent for TDG at a temperature of 150oC and 10 MPa.
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